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TETRAKIS(DIMETHYLAMINO)DIBORON

  • CAS No.:1630-79-1
  • Purity:99%
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Factory Sells Best Quality TETRAKIS(DIMETHYLAMINO)DIBORON 1630-79-1 with steady supply

  • Molecular Formula:C8H24 B2 N4
  • Molecular Weight:197.927
  • Vapor Pressure:0.163mmHg at 25°C 
  • Melting Point:-33°C(lit.) 
  • Refractive Index:n20/D 1.4750(lit.) 
  • Boiling Point:213.6°Cat760mmHg 
  • PKA:-0.25±0.70(Predicted) 
  • Flash Point:83°C 
  • PSA:12.96000 
  • Density:0.847g/cm3 
  • LogP:-0.71240 

TETRAKIS(DIMETHYLAMINO)DIBORON(Cas 1630-79-1) Usage

Synthesis Reference(s)

Journal of the American Chemical Society, 82, p. 6242, 1960 DOI: 10.1021/ja01509a009

InChI:InChI=1/C8H24B2N4/c1-11(2)9(12(3)4)10(13(5)6)14(7)8/h1-8H3

1630-79-1 Relevant articles

Synthetic routes to cyclic and unsymmetric diborane(4) compounds

Lesley, M.J. Gerald,Norman, Nicholas C.,Orpen, A. Guy,Starbuck, Jonathan

, p. 115 - 117 (2007/10/03)

The reaction between 1,2-B2Cl2(NMe2)2 an...

Contribution to the Chemistry of Boron, 224 Reactions and Structure of Electron-Precise Triborane(5) and Tetraborane(6) Derivatives

Linti, Gerald,Loderer, Dirk,Noeth, Heinrich,Polborn, Kurt,Rattay, Wilfried

, p. 1909 - 1922 (2007/10/02)

An improved synthesis of B3(NMe2)5 (2), ...

1630-79-1 Process route

diboron tetrachloride
13701-67-2

diboron tetrachloride

dimethyl amine
124-40-3

dimethyl amine

tetrakis(dimethylamido)diborane
1630-79-1

tetrakis(dimethylamido)diborane

N,N-dimethylammonium chloride
506-59-2

N,N-dimethylammonium chloride

Conditions
Conditions Yield
Tris-dimethylamino-diborbromid
92473-84-2

Tris-dimethylamino-diborbromid

tetrakis(dimethylamido)diborane
1630-79-1

tetrakis(dimethylamido)diborane

tris(dimethylamino)borane
4375-83-1

tris(dimethylamino)borane

hexakis(dimethylamino)tetraborane<sup>(6)</sup>
26459-63-2

hexakis(dimethylamino)tetraborane(6)

Conditions
Conditions Yield
With NaK2.8; In pentane; byproducts: NaBr, KBr; anhydrous and oxygen-free condns., addn. of B-compd. in pentane to alloy in pentane in such manner, that refluxing maintained for 5 h, refluxed for 3 h with stirring; filtered, pentane removed in vac., fractional distn.;
38%

1630-79-1 Upstream products

  • 13701-67-2
    13701-67-2

    diboron tetrachloride

  • 124-40-3
    124-40-3

    dimethyl amine

  • 15631-70-6
    15631-70-6

    {(CH3)2N}2BMn(CO)5

  • 92473-84-2
    92473-84-2

    Tris-dimethylamino-diborbromid

1630-79-1 Downstream products

  • 106506-15-4
    106506-15-4

    Tetrakis--diboran

  • 13826-23-8
    13826-23-8

    Tetraphenoxy-dibor

  • 1201-45-2
    1201-45-2

    Bis-(dimethylamino)-phenylboran

  • 73183-34-3
    73183-34-3

    bis(pinacol)diborane

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